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High Purity 99% 1-Butylsulfonyl Chloride Cas 2386-60-9 1-Butanesulfonyl Chloride

2023-09-26

Chemical Properties:clear colourless to light yellow liquid;

CAS 2386-60-9 Uses

1-Butanesulfonyl chloride has been used in the preparation of:(1)ethyl 2-(1-butanesulfonamido)pent-4-yn-l-oate

(2)1-butanesulfonamid-N,N′-1,2-ethanediylbis

(3)1-butanesulfonamide-N,N′-1,3-propanediylbis

Purification Methods

It has a pungent odour and is LACHRYMATORY.  If IR shows OH bands, then dissolve in Et2O, wash with cold saturated aqueous NaHCO3 (care since CO2 will be generated) then H2O, dry it over solid Na2SO4, filter, evaporate and distil the residue twice.  Characterise it by shaking a solution in Et2O or *C6H6 with aqueous NH3, collect the solid 1-butanesulfonamide with m 48o after recrystallisation from CHCl3, CCl4 or Et2O/pet ether.  

CAS 2386-60-9
Application for medicine and pesticide intermediates
Appearance light yellow oily liquid, with pungent odor
Melting Point -29°C
Boiling Point 80-81°C (9mmHg)
Density 1.208 g/ml at 25°C
Refractive Index 1.454
Flash Point 79°C
Moisture ≤0.2%